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Diels-Alder Reaction of cis-Butadiene with Maleic Anhydride Experiment: Give the reaction conditions, ie. what apparatus, solvent, temperature and...

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Chemistry

Diels-Alder Reaction of cis-Butadiene with MaleicAnhydride Experiment:

Give the reaction conditions, ie. what apparatus, solvent,temperature and time will be used. How will the product be isolatedfrom the reaction mixture and how will it be characterized?

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4.3 Ratings (629 Votes)
Experimental SetUp for DielsAlderReactionThe 25mL round bottom flask contained 279 grams of3sulfolene 163 grams of maleic anhydride and 10 mL of xyleneto dissolve the materials The solution was lightly heated untilthe mixture fully dissolved then the mixture was strongly heateduntil reflux The reaction was conducted at reflux temperature for30 minutes After the round bottom flask was removed from theexperimental setup 10 mL of xylene was added to the hot mixtureand the reaction was stirred until all    See Answer
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